8WXR
Structure of WDR5 in complex with WIN motif containing MBD3C F47A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 64.697, 47.028, 103.050 |
Unit cell angles | 90.00, 107.47, 90.00 |
Refinement procedure
Resolution | 12.650 - 2.080 |
R-factor | 0.1572 |
Rwork | 0.153 |
R-free | 0.19860 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.022 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.140 |
High resolution limit [Å] | 2.080 | 2.100 |
Rmerge | 0.051 | 0.181 |
Number of reflections | 31841 | 1443 |
<I/σ(I)> | 16.52 | |
Completeness [%] | 90.3 | |
Redundancy | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2 M potassium dihydrogen phosphate, 20% PEG 3350 |