8WIK
Crystal structure of human FSP1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2023-01-15 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 56.875, 56.875, 505.105 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.260 - 2.000 |
R-factor | 0.227 |
Rwork | 0.225 |
R-free | 0.26270 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.943 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 4.310 | 2.000 |
Rmerge | 0.118 | 0.072 | 1.621 |
Rmeas | 0.125 | 0.076 | 1.718 |
Rpim | 0.040 | 0.026 | 0.559 |
Total number of observations | 339711 | ||
Number of reflections | 34829 | 3969 | 3353 |
<I/σ(I)> | 4.6 | ||
Completeness [%] | 100.0 | 99.9 | 100 |
Redundancy | 9.8 | 8.8 | 9.2 |
CC(1/2) | 0.969 | 0.989 | 0.530 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | HEPES , MgCl2, PEG3350 |