8VPX

UIC-10-BPE extension of UIC-1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-D
Synchrotron site	APS
Beamline	21-ID-D
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-09-24
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.688839
Spacegroup name	P 1
Unit cell lengths	10.305, 17.610, 26.616
Unit cell angles	99.46, 99.72, 95.85

Refinement procedure

Resolution	17.220 - 1.451
R-factor	0.1299
Rwork	0.123
R-free	0.18140
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	1.641
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	17.220	1.502
High resolution limit [Å]	1.451	1.451
Number of reflections	2572	173
<I/σ(I)>	28.56
Completeness [%]	80.2
Redundancy	3.7
CC(1/2)	0.999	0.997

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	SLOW COOLING		298	Methanol, acetonitrile, water