8VPE
UIC-10-BIF extension of UIC-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-10-28 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.6199 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 10.764, 36.020, 47.455 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 16.840 - 0.910 |
R-factor | 0.0965 |
Rwork | 0.095 |
R-free | 0.11140 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.938 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 16.840 | 0.943 |
High resolution limit [Å] | 0.910 | 0.910 |
Number of reflections | 13878 | 1314 |
<I/σ(I)> | 21.69 | |
Completeness [%] | 99.2 | |
Redundancy | 12.8 | |
CC(1/2) | 0.998 | 0.979 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SLOW COOLING | 298 | Acetonitrile, water |