8VFD
Ternary DNA Polymerase Beta bound to DNA containing template FapydG incoming TTP analog
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-06-16 |
Detector | DECTRIS PILATUS3 R 200K-A |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.770, 79.070, 54.366 |
Unit cell angles | 90.00, 107.91, 90.00 |
Refinement procedure
Resolution | 25.020 - 2.100 |
R-factor | 0.2034 |
Rwork | 0.200 |
R-free | 0.24220 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.110 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.020 | 2.140 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 32606 | 1233 |
<I/σ(I)> | 18.9 | |
Completeness [%] | 99.5 | |
Redundancy | 4 | |
CC(1/2) | 0.999 | 0.428 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 14-22% PEG 3350 0.05 M Imidazole pH 8.0 0.35 M Sodium Acetate |