8VCY
Human TCR A2.13 in complex with DQ8-InsC8-15NPY
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-09-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.95373 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 67.803, 106.695, 132.962 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.510 - 2.600 |
R-factor | 0.1865 |
Rwork | 0.184 |
R-free | 0.22500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.493 |
Data reduction software | autoXDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.19_4092) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.510 | 2.720 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.102 | 0.349 |
Rmeas | 0.112 | |
Rpim | 0.046 | 0.109 |
Number of reflections | 30434 | 3659 |
<I/σ(I)> | 16.5 | 7.8 |
Completeness [%] | 100.0 | |
Redundancy | 10.6 | |
CC(1/2) | 0.995 | 0.982 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293.15 | 0.2 M Potassium sodium tartrate, 14% PEG 20,000 with seeding C8 silver bullet (Hampton Research) |