8V8M
Switchgrass Chalcone Synthase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.1 |
Synchrotron site | ALS |
Beamline | 5.0.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-11-11 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 1 |
Spacegroup name | P 1 |
Unit cell lengths | 51.050, 83.085, 106.450 |
Unit cell angles | 79.43, 76.25, 77.21 |
Refinement procedure
Resolution | 48.720 - 1.820 |
R-factor | 0.2644 |
Rwork | 0.264 |
R-free | 0.28860 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.782 |
Data reduction software | DIALS |
Data scaling software | DIALS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.20_4459: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.720 | 1.885 |
High resolution limit [Å] | 1.820 | 1.820 |
Rmerge | 0.145 | 0.605 |
Number of reflections | 233811 | 21963 |
<I/σ(I)> | 4.43 | 0.88 |
Completeness [%] | 93.4 | 91.22 |
Redundancy | 1.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.2 M Sodium Formate, 20% PEG 3350 |