8V7H
Human DNA polymerase eta-DNA-araC-ended primer ternary complex:ground state at pH7.0 (K+ MES) with 1 Ca2+ ion
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-D |
Synchrotron site | APS |
Beamline | 21-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-09-16 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.12723 |
Spacegroup name | P 61 |
Unit cell lengths | 98.403, 98.403, 81.574 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.770 - 1.680 |
R-factor | 0.2093 |
Rwork | 0.208 |
R-free | 0.23290 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.139 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 37.770 | 37.770 | 1.790 |
High resolution limit [Å] | 1.680 | 5.030 | 1.680 |
Rmerge | 0.046 | 0.027 | 0.819 |
Rmeas | 0.048 | 0.029 | 0.862 |
Number of reflections | 50730 | 3757 | 16115 |
<I/σ(I)> | 25.27 | ||
Completeness [%] | 100.0 | ||
Redundancy | 20.4 | ||
CC(1/2) | 1.000 | 0.999 | 0.858 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | PEG 2000MME, 0.1 M MES |