8U08
Crystal structure of 10E8-GT11 scaffold in complex with a human 10E8 inferred germline (10E8-iGL1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-10-15 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 69.749, 73.905, 129.882 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.780 - 1.980 |
R-factor | 0.1886 |
Rwork | 0.186 |
R-free | 0.23580 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.131 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.800 | 2.010 |
High resolution limit [Å] | 1.980 | 1.980 |
Rpim | 0.052 | 0.412 |
Number of reflections | 43220 | 1662 |
<I/σ(I)> | 13 | 1.2 |
Completeness [%] | 92.1 | 70.8 |
Redundancy | 7.9 | 5.6 |
CC(1/2) | 0.850 | 0.430 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.095 M NaCitrate,19% 2-propanol, 5% glycerol, 19% PEG4000 |