8TY7
Crystal structure of 05.GC.w2.3C10 Fab in complex with H1 HA from A/California/04/2009(H1N1)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-1 |
Synchrotron site | SSRL |
Beamline | BL12-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-11-03 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9795 |
Spacegroup name | I 21 3 |
Unit cell lengths | 201.006, 201.006, 201.006 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.030 - 3.210 |
R-factor | 0.247 |
Rwork | 0.244 |
R-free | 0.28840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4m4y |
RMSD bond length | 0.002 |
RMSD bond angle | 0.438 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.900 | 3.260 |
High resolution limit [Å] | 3.210 | 3.210 |
Rpim | 0.044 | |
Number of reflections | 22209 | 2179 |
<I/σ(I)> | 22 | 0.6 |
Completeness [%] | 100.0 | 100 |
Redundancy | 22.1 | |
CC(1/2) | 0.998 | 0.230 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2 M sodium acetate, pH 6.4, 18% PEG3350 |