8TTU
Structure of SNX27 FERM complexed with Fam21A repeat 19 (1261 - 1274)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-09-24 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.953700 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.544, 74.497, 102.529 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.250 - 2.360 |
R-factor | 0.2036 |
Rwork | 0.198 |
R-free | 0.25120 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.093 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.540 | 2.450 |
High resolution limit [Å] | 2.360 | 2.360 |
Rmerge | 0.097 | 0.545 |
Rmeas | 0.109 | 0.608 |
Rpim | 0.048 | 0.263 |
Total number of observations | 64599 | 6238 |
Number of reflections | 12319 | 1195 |
<I/σ(I)> | 8.4 | 1.7 |
Completeness [%] | 98.8 | |
Redundancy | 5.2 | 5.2 |
CC(1/2) | 0.995 | 0.801 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1 M Sodium Cacodylate pH 6.5 and 25% PEG3350 |