8TTT
Structure of SNX27 FERM complexed with Fam21A repeat 15 (1124-1140)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-10-24 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.953700 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.567, 74.371, 105.229 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.950 - 2.350 |
R-factor | 0.1968 |
Rwork | 0.191 |
R-free | 0.25090 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.054 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.950 | 2.410 |
High resolution limit [Å] | 2.330 | 2.330 |
Rmerge | 0.203 | 1.524 |
Rmeas | 0.220 | 1.656 |
Rpim | 0.083 | 0.632 |
Total number of observations | 88510 | 5906 |
Number of reflections | 12909 | 940 |
<I/σ(I)> | 7.9 | 1.1 |
Completeness [%] | 97.6 | |
Redundancy | 6.9 | 6.3 |
CC(1/2) | 0.995 | 0.379 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 0.1 M Sodium Cacodylate pH 6.0 and 22.5% PEG4000 |