8TJ8
CRYSTAL STRUCTURE OF THE A/Moscow/10/1999(H3N2) INFLUENZA VIRUS HEMAGGLUTININ WITH HUMAN RECEPTOR ANALOG 6'-SLNLN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-07 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.03317 |
Spacegroup name | H 3 2 |
Unit cell lengths | 100.031, 100.031, 385.290 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.040 - 2.560 |
R-factor | 0.217 |
Rwork | 0.209 |
R-free | 0.25760 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.703 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.040 | 2.640 |
High resolution limit [Å] | 2.550 | 2.550 |
Rpim | 0.040 | 0.330 |
Number of reflections | 24519 | 2399 |
<I/σ(I)> | 17.9 | 1.6 |
Completeness [%] | 100.0 | |
Redundancy | 9.2 | |
CC(1/2) | 0.998 | 0.904 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 40% PEG-400 and 0.2 M Calcium acetate, 0.1M HEPES pH 7.5 |