8T8T
Crystal structure of TET25 in complex with PyDH2 ligand in P212121 space group
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 183 |
Detector technology | PIXEL |
Collection date | 2023-02-24 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9791 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 29.624, 51.923, 88.064 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.960 - 1.620 |
R-factor | 0.2081 |
Rwork | 0.207 |
R-free | 0.22790 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.311 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX (1.19.2_4158) |
Refinement software | PHENIX (1.21.1_5286) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.960 | 1.650 |
High resolution limit [Å] | 1.620 | 1.620 |
Rmerge | 0.103 | |
Number of reflections | 8871 | 343 |
<I/σ(I)> | 8.8 | 0.8 |
Completeness [%] | 98.4 | 73.3 |
Redundancy | 12.8 | 12.6 |
CC(1/2) | 0.999 | 0.530 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | 0.05 M KCl, 0.1 M LiCl, 0.012 M spermine tetrahydrochloride, 0.05 M MES pH 6.5, 25% v/v PEG 400 |