8SZP
Human DHX9 bound to ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-05-05 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.97624 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 119.100, 122.260, 349.180 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 59.621 - 2.620 |
Rwork | 0.219 |
R-free | 0.27360 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.877 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0405) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.130 | 2.670 |
High resolution limit [Å] | 2.620 | 2.620 |
Rmerge | 0.062 | 1.398 |
Rmeas | 0.064 | 1.450 |
Rpim | 0.018 | 0.382 |
Total number of observations | 980269 | 63231 |
Number of reflections | 76541 | 4516 |
<I/σ(I)> | 21.8 | 2.2 |
Completeness [%] | 99.7 | |
Redundancy | 12.8 | 14 |
CC(1/2) | 1.000 | 0.815 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 291 | 200 mM Lithium sulfate, 100 mM MES pH 6, 20% (w/v) PEG 4000; 5 mM ADP and 50 mM magnesium chloride in protein solution |