8SX0
Bordetella filamentous hemagglutinin (FhaB) C-terminal domain
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-03-28 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795, 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 23.060, 46.576, 75.987 |
Unit cell angles | 90.00, 91.69, 90.00 |
Refinement procedure
Resolution | 39.710 - 1.650 |
R-factor | 0.1815 |
Rwork | 0.179 |
R-free | 0.20430 |
Structure solution method | MAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.080 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | AutoSol |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.580 | 1.680 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.060 | 0.805 |
Rmeas | 0.071 | 0.952 |
Rpim | 0.038 | 0.501 |
Number of reflections | 19264 | 962 |
<I/σ(I)> | 15 | 2.2 |
Completeness [%] | 98.8 | 99.6 |
Redundancy | 6.7 | 6.9 |
CC(1/2) | 0.999 | 0.704 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1 M phosphate citrate pH 5, 26.5% PEG 8000, 0.2 M NaCl |