8S8V
OPR3 variant R283D in its monomeric form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-02-08 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 0.87 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 86.390, 89.314, 95.528 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.660 - 3.000 |
R-factor | 0.2545 |
Rwork | 0.250 |
R-free | 0.29660 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.034 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.21_5207: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.660 | 2.760 |
High resolution limit [Å] | 2.690 | 2.690 |
Rpim | 0.290 | 0.890 |
Number of reflections | 133610 | 37427 |
<I/σ(I)> | 1.71 | |
Completeness [%] | 94.4 | |
Redundancy | 3.6 | |
CC(1/2) | 0.900 | 0.180 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.1 M MES/Tris (6.5), 10 mM ammonium sulfate, 8-16% PEG8000 |