8S6Y

Co-crystal structure of TEAD1 with OPN-9652

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-1
Synchrotron site	ESRF
Beamline	ID23-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-01-26
Detector	DECTRIS EIGER2 X CdTe 16M
Wavelength(s)	0.885603
Spacegroup name	P 32 2 1
Unit cell lengths	120.957, 120.957, 155.520
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	104.752 - 2.031
Rwork	0.223
R-free	0.25810
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	1.336
Data reduction software	autoPROC
Data scaling software	autoPROC
Phasing software	PHASER
Refinement software	REFMAC (5.8.0267)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	104.752	2.066
High resolution limit [Å]	2.031	2.031
Number of reflections	81249	3241
<I/σ(I)>	6.5
Completeness [%]	95.4
Redundancy	12.6
CC(1/2)	0.990	0.664

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		293	buffer, salt and precipitant