8RNH
Crystal structure of HLA B*18:01 in complex with EEIEITTHF, an 9-mer epitope from Influenza A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-07-30 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.953732 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.750, 81.627, 110.556 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.120 - 1.600 |
R-factor | 0.2033 |
Rwork | 0.202 |
R-free | 0.23450 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.916 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.120 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 59129 | 3078 |
<I/σ(I)> | 10.3 | 1.6 |
Completeness [%] | 97.0 | |
Redundancy | 4.7 | |
CC(1/2) | 0.997 | 0.630 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M Lithium Acetate, 20% w/v PEG 3350, and 10 mM MgCl2 |