Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-06-18 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.000002 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 44.633, 129.220, 37.670 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 42.190 - 1.560 |
| R-factor | 0.1735 |
| Rwork | 0.171 |
| R-free | 0.22510 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.122 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (dev_5246) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.190 | 1.640 |
| High resolution limit [Å] | 1.560 | 1.560 |
| Rmeas | 0.143 | 1.460 |
| Number of reflections | 60215 | 9679 |
| <I/σ(I)> | 8.67 | 1.31 |
| Completeness [%] | 99.8 | 99.7 |
| Redundancy | 5.7 | 5.4 |
| CC(1/2) | 0.997 | 0.665 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.1M BisTris Propane pH 6.5, 0.2 M NaNO3, 20% w/v PEG3350, 10% ethylene glycol |
