8RIT
Dimeric mutant S103D of the BTB domain of ZBTB8A from Xenopus laevis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-11-25 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.98012 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 259.993, 61.993, 71.488 |
Unit cell angles | 90.00, 91.52, 90.00 |
Refinement procedure
Resolution | 71.460 - 3.750 |
R-factor | 0.2464 |
Rwork | 0.244 |
R-free | 0.29540 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.001 |
RMSD bond angle | 0.307 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 129.960 | 3.810 |
High resolution limit [Å] | 3.750 | 3.750 |
Rpim | 0.129 | 0.777 |
Number of reflections | 11929 | 547 |
<I/σ(I)> | 4.5 | 1.2 |
Completeness [%] | 99.7 | 93.7 |
Redundancy | 6.5 | |
CC(1/2) | 0.914 | 0.798 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | MDL MORPHEUS I 1.38 (Alcohols, Buffer 1, EDO_P8K) |