8RGU
Arginase 2 in complex with inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU300 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-04-15 |
| Detector | RIGAKU SATURN A200 |
| Wavelength(s) | 1.541 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 48.281, 134.119, 144.125 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 98.180 - 1.900 |
| Rwork | 0.205 |
| R-free | 0.24630 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 144.130 | 2.000 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.073 | 0.520 |
| Number of reflections | 74744 | 6000 |
| <I/σ(I)> | 16.3 | |
| Completeness [%] | 100.0 | |
| Redundancy | 5.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 13-18% PEG3350, 0.2-0.35M Am.Cit. pH7.0 |
