8RD1
HUWE1 WWE domain in complex with compound 4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-08-20 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.000000 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 62.768, 62.768, 231.456 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.980 - 1.896 |
R-factor | 0.181 |
Rwork | 0.179 |
R-free | 0.21970 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.920 |
Data scaling software | STARANISO ((Version 1.1.7)) |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.8) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.580 | 1.928 |
High resolution limit [Å] | 1.896 | 1.896 |
Rmerge | 0.135 | |
Number of reflections | 38225 | 532 |
<I/σ(I)> | 13.4 | 1.4 |
Completeness [%] | 93.2 | 30.6 |
Redundancy | 12.7 | 8.1 |
CC(1/2) | 0.998 | 0.647 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 278 | 0.1 M Na Acetate pH 4.83, 2.9 M NaCl |