8R9B
A soakable crystal form of human CDK7 in complex with AMP-PNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-11-19 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.99987 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 76.140, 180.285, 76.335 |
Unit cell angles | 90.00, 117.85, 90.00 |
Refinement procedure
Resolution | 90.140 - 2.210 |
R-factor | 0.19491 |
Rwork | 0.192 |
R-free | 0.24265 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.011 |
RMSD bond angle | 1.547 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 90.140 | 2.391 |
High resolution limit [Å] | 2.210 | 2.260 |
Rmeas | 0.091 | 1.048 |
Number of reflections | 64931 | 3316 |
<I/σ(I)> | 10.5 | 1.7 |
Completeness [%] | 86.1 | 47 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 277 | 19% 2-propanol, 5% glycerol, 19%PEG4K, 0.095M Na3citrate pH5.6/HCl |