8R99
A soakable crystal form of human CDK7 in complex with AMP-PNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-30 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97625 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 144.872, 40.232, 68.589 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.520 - 1.810 |
R-factor | 0.17757 |
Rwork | 0.175 |
R-free | 0.21980 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.009 |
RMSD bond angle | 1.393 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.436 | 1.951 |
High resolution limit [Å] | 1.809 | 1.809 |
Rmeas | 0.068 | 1.180 |
Number of reflections | 24282 | 1214 |
<I/σ(I)> | 13.31 | 1.2 |
Completeness [%] | 91.8 | |
Redundancy | 5.62 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | .1M (NH4)3 citrate .2M NDSB-201 15.2% PEG 3350 |