8R7O
HUWE1 WWE domain in complex with 2'F-ATP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-11-15 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.999824 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 62.915, 62.915, 231.945 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.640 - 1.360 |
R-factor | 0.1693 |
Rwork | 0.168 |
R-free | 0.19510 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.229 |
Data reduction software | XDS ((VERSION Feb 5) |
Data scaling software | autoPROC ((Version 1.1.7)) |
Phasing software | PHASER |
Refinement software | PHENIX (1.21_5207) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.721 | 1.450 |
High resolution limit [Å] | 1.360 | 1.361 |
Rmerge | 0.060 | |
Number of reflections | 86990 | 4348 |
<I/σ(I)> | 23.2 | |
Completeness [%] | 86.2 | 25.4 |
Redundancy | 20 | |
CC(1/2) | 0.999 | 0.649 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 278 | 0.1 M Na Acetate pH 4.83, 2.9 M NaCl |