8R79
The D2 domain of human DTX3L
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I23 |
Synchrotron site | Diamond |
Beamline | I23 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2021-10-22 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 2.7552 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 140.893, 140.893, 41.037 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 70.450 - 2.180 |
R-factor | 0.21428 |
Rwork | 0.210 |
R-free | 0.24885 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.509 |
Data reduction software | autoPROC |
Data scaling software | XSCALE |
Phasing software | HKL2Map |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 70.450 | 2.334 |
High resolution limit [Å] | 2.180 | 2.181 |
Rmerge | 0.107 | |
Number of reflections | 12554 | 628 |
<I/σ(I)> | 33.3 | 1.7 |
Completeness [%] | 91.7 | 67.2 |
Redundancy | 90.6 | 55.2 |
CC(1/2) | 1.000 | 0.842 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.3 | 294 | 2.2 M (NH4)2SO4, 100 mM BisTris |