8QOY
Capsular polysaccharide synthesis multienzyme of Actinobacillus Pleuropneumoniae serotype 3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-11-18 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.67 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 207.911, 207.911, 93.659 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.550 - 3.000 |
R-factor | 0.1845 |
Rwork | 0.183 |
R-free | 0.22080 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.489 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.550 | 3.107 |
High resolution limit [Å] | 3.000 | 3.000 |
Number of reflections | 46791 | 4630 |
<I/σ(I)> | 9.23 | |
Completeness [%] | 99.9 | |
Redundancy | 62.5 | |
CC(1/2) | 0.998 | 0.936 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 291 | 1.6 M magnesium sulphate heptahydrate, 0.1 M MES pH 6.5 |