8QJS
VHL/Elongin B/Elongin C complex with compound 155
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-23 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9121 |
Spacegroup name | P 41 2 2 |
Unit cell lengths | 93.235, 93.235, 361.904 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.740 - 3.191 |
R-factor | 0.2552 |
Rwork | 0.254 |
R-free | 0.27410 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.870 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.8 (8-JUN-2022)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.760 | 3.250 |
High resolution limit [Å] | 3.018 | 3.018 |
Rmerge | 0.160 | 0.861 |
Number of reflections | 27684 | 1355 |
<I/σ(I)> | 13.1 | 3.1 |
Completeness [%] | 100.0 | |
Redundancy | 13 | |
CC(1/2) | 0.999 | 1.000 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 291 | 100 mM Sodium Citrate pH 6.0, 200 mM Magnesium Acetate, 50 mM DTT, 14% PEG 8000 |