8QJ4
Receptor Sd-Amt1 (ON-state)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-12-25 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1 |
Spacegroup name | H 3 |
Unit cell lengths | 115.098, 115.098, 275.718 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.090 - 1.700 |
R-factor | 0.15063 |
Rwork | 0.150 |
R-free | 0.16615 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.710 |
Data reduction software | HKL-2000 |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0419) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.780 |
High resolution limit [Å] | 1.650 | 1.750 |
Rmerge | 0.106 | 1.693 |
Rmeas | 0.112 | 1.803 |
Rpim | 0.035 | 0.614 |
Total number of observations | 57709 | |
Number of reflections | 137206 | 6813 |
<I/σ(I)> | 13.2 | 1.3 |
Completeness [%] | 100.0 | |
Redundancy | 10.3 | 8.5 |
CC(1/2) | 0.999 | 0.529 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 0.1 M Bis/Tris pH 6.5 with 25 % (w/v) PEG 3350 |