Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
| Synchrotron site | PETRA III, EMBL c/o DESY |
| Beamline | P14 (MX2) |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-06-27 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.9763 |
| Spacegroup name | P 1 |
| Unit cell lengths | 45.727, 53.611, 100.770 |
| Unit cell angles | 90.03, 90.02, 64.79 |
Refinement procedure
| Resolution | 27.620 - 1.225 |
| Rwork | 0.168 |
| R-free | 0.19240 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 27.620 | 1.269 |
| High resolution limit [Å] | 1.225 | 1.225 |
| Rmerge | 0.061 | 0.378 |
| Number of reflections | 245404 | 9517 |
| <I/σ(I)> | 16.05 | |
| Completeness [%] | 84.0 | |
| Redundancy | 6.7 | |
| CC(1/2) | 0.999 | 0.886 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 292 | Morpheus Screen I, condition A4 |
