8Q5R
HpARI bound to mouse IL-33
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-05-29 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.9795 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 149.779, 35.755, 61.289 |
Unit cell angles | 90.00, 92.07, 90.00 |
Refinement procedure
Resolution | 48.260 - 2.100 |
R-factor | 0.1839 |
Rwork | 0.180 |
R-free | 0.23000 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | DIALS |
Data scaling software | DIALS |
Phasing software | PHASER |
Refinement software | BUSTER |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.260 | 2.140 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 19343 | 1046 |
<I/σ(I)> | 13.1 | |
Completeness [%] | 100.0 | |
Redundancy | 6.8 | |
CC(1/2) | 0.998 | 0.728 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.1 M Bis-Tris pH 6.8 and 22% PEG3350 |