8PW0
Manganese-dependent transcriptional repressor DR2539 complexed with manganese and bound to dr1709 promotor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.976250 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 67.710, 67.710, 158.137 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.880 - 2.200 |
R-factor | 0.1849 |
Rwork | 0.183 |
R-free | 0.22730 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.095 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.880 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 19507 | 2768 |
<I/σ(I)> | 13.1 | |
Completeness [%] | 100.0 | |
Redundancy | 8.8 | |
CC(1/2) | 0.998 | 0.678 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 8K 26% (w/v); Imidazole 0.1 M pH 7.8; NaCl 0.2 M |