8PO5

Lactobacillus plantarum LpdD

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04-1
Synchrotron site	Diamond
Beamline	I04-1
Temperature [K]	80
Detector technology	PIXEL
Collection date	2018-01-21
Detector	DECTRIS EIGER2 S 9M
Wavelength(s)	0.987
Spacegroup name	I 2 2 2
Unit cell lengths	53.500, 92.980, 126.820
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	75.033 - 2.100
R-factor	0.197
Rwork	0.195
R-free	0.25180
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.866
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.14_3260)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	75.033	2.175
High resolution limit [Å]	2.100	2.100
Number of reflections	18833	1841
<I/σ(I)>	9.83
Completeness [%]	99.7
Redundancy	2
CC(1/2)	1.000	0.900

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.1M Tris-Cl pH8.5, 0.2M Magnesium chloride, 30% PEG4K