Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 298 |
Detector technology | AREA DETECTOR |
Collection date | 1992-04 |
Detector | SIEMENS |
Spacegroup name | P 65 |
Unit cell lengths | 50.060, 50.060, 98.720 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 26.200 - 1.600 |
R-factor | 0.167 * |
Structure solution method | KNOWN |
RMSD bond length | 0.007 |
RMSD bond angle | 0.019 |
Data reduction software | XENGEN |
Data scaling software | XENGEN |
Refinement software | SHELXL |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.200 | 1.700 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.044 * | 0.150 |
Number of reflections | 18528 | |
<I/σ(I)> | 20.6 | 5.8 |
Completeness [%] | 88.0 * | 65 * |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 50MM SODIUM PHOSPHATE WITH 75% SATURATED AMMONIUM SULFATE., pH 6.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | 50 (mM) | ||
2 | 1 | 1 | ammonium sulfate | 75 (%sat) |