8PAS
Crystal structure of MAP4K1 with a SMOL inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.99998 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 61.040, 100.056, 61.055 |
Unit cell angles | 90.00, 102.03, 90.00 |
Refinement procedure
Resolution | 42.910 - 2.700 |
R-factor | 0.23093 |
Rwork | 0.228 |
R-free | 0.29970 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.887 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.910 | 2.950 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmeas | 0.049 | 0.529 |
Number of reflections | 19051 | 4477 |
<I/σ(I)> | 21.55 | 3.5 |
Completeness [%] | 96.1 | 97 |
Redundancy | 3 | 3.1 |
CC(1/2) | 0.999 | 0.936 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | NOT DISCLOSED |