8P90
TARGET COMPLEX 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 11.2C |
Synchrotron site | ELETTRA |
Beamline | 11.2C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-07-31 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.000 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 94.657, 94.657, 441.848 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.280 - 2.800 |
R-factor | 0.2718 |
Rwork | 0.271 |
R-free | 0.29540 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.450 |
Data reduction software | XDS |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.280 | 3.480 |
High resolution limit [Å] | 2.740 | 2.740 |
Rmerge | 0.360 | |
Number of reflections | 32276 | 3913 |
<I/σ(I)> | 4.7 | |
Completeness [%] | 100.0 | |
Redundancy | 10.1 | |
CC(1/2) | 0.300 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 293 | 1 M LITHIUM SULFATE |