8OWY
Crystal structure of METTL6 mutant 40-269 bound to SAH
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-12-01 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.008 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 81.971, 138.129, 39.660 |
Unit cell angles | 90.00, 115.26, 90.00 |
Refinement procedure
Resolution | 39.110 - 3.200 |
R-factor | 0.2619 |
Rwork | 0.260 |
R-free | 0.29960 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 2.041 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.16_3549: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.110 | 3.315 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.205 | 2.196 |
Number of reflections | 6561 | 318 |
<I/σ(I)> | 6.97 | |
Completeness [%] | 85.3 | |
Redundancy | 6.5 | |
CC(1/2) | 0.995 | 0.861 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 0.1 M BisTRIS, 0.2 M ammonium sulfate and 25% PEG3350 |