8OV5

PERIDININ-CHLOROPHYLL-PROTEIN OF AMPHIDINIUM CARTERAE, 100K

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	CCD
Collection date	2007-02-04
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	0.9796
Spacegroup name	C 1 2 1
Unit cell lengths	197.140, 115.610, 65.880
Unit cell angles	90.00, 94.97, 90.00

Refinement procedure

Resolution	43.380 - 1.150
R-factor	0.1414
Rwork	0.141
R-free	0.15470
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.012
RMSD bond angle	1.181
Data reduction software	XDS (VERSION Feb 5, 2021 BUILT=20210323)
Data scaling software	XSCALE (VERSION Feb 5, 2021 BUILT=20210323)
Phasing software	PHENIX (1.20.1_4487)
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.820	1.180
High resolution limit [Å]	1.150	1.150
Rmerge	0.044	0.833
Rmeas	0.050	1.111
Number of reflections	444109	12493
<I/σ(I)>	13.33	1.01
Completeness [%]	85.6	32.6
Redundancy	3.5
CC(1/2)	0.999	0.440

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	291	14% PEG8000, 100mM Tris-HCL pH 7.5, 200mM MgCl2