8OK4

Variant Surface Glycoprotein VSG11wt-Oil

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-09-03
Detector	DECTRIS PILATUS 2M-F
Wavelength(s)	1
Spacegroup name	P 3 2 1
Unit cell lengths	74.862, 74.862, 105.611
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	40.940 - 1.230
R-factor	0.1631
Rwork	0.162
R-free	0.18840
Structure solution method	SAD
Data reduction software	xia2
Data scaling software	Aimless
Phasing software	SHELX
Refinement software	PHENIX (1.19.2-4158)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.940	1.274
High resolution limit [Å]	1.230	1.230
Rmerge	0.075	1.777
Number of reflections	99764	9827
<I/σ(I)>	15.79	0.98
Completeness [%]	99.9
Redundancy	9.4
CC(1/2)	1.000	0.748

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8.5	296	1.7 M NaKTartrate, 100 mM Tris/HCl