8K1F

Crystal Structure of TrmR from Fusobacterium nucleatum

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Temperature [K]	100
Detector technology	CCD
Collection date	2022-06-06
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.0
Spacegroup name	C 1 2 1
Unit cell lengths	165.281, 46.589, 87.316
Unit cell angles	90.00, 98.33, 90.00

Refinement procedure

Resolution	36.097 - 2.400
R-factor	0.2206
Rwork	0.213
R-free	0.29230
Structure solution method	SAD
RMSD bond length	0.009
RMSD bond angle	0.947
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.15.2_3472: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	36.100	2.486
High resolution limit [Å]	2.400	2.400
Number of reflections	110870	23951
<I/σ(I)>	11.2
Completeness [%]	80.8
Redundancy	4.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6	295	0.1M MES, 9% PEG 8000, 95mM calcium acetate