8K0J
Crystal structure of Cas7f
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-07-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | P 61 |
Unit cell lengths | 100.516, 100.516, 54.669 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 36.999 - 2.365 |
R-factor | 0.194 |
Rwork | 0.193 |
R-free | 0.22190 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.503 |
Data reduction software | HKL-3000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.450 |
High resolution limit [Å] | 2.365 | 2.365 |
Rmerge | 0.146 | 0.155 |
Number of reflections | 12986 | 1284 |
<I/σ(I)> | 32.9 | |
Completeness [%] | 99.7 | |
Redundancy | 14.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 400, Sodium chloride |