8K0H
Structure of Cas5f-8f
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-03-13 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.575, 68.186, 73.631 |
Unit cell angles | 90.00, 109.72, 90.00 |
Refinement procedure
Resolution | 46.692 - 2.560 |
R-factor | 0.1941 |
Rwork | 0.192 |
R-free | 0.23380 |
Structure solution method | SAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.707 |
Data reduction software | HKL-3000 |
Data scaling software | SCALEPACK |
Phasing software | AutoSol |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.650 |
High resolution limit [Å] | 2.560 | 2.560 |
Rmerge | 0.141 | 0.645 |
Number of reflections | 14740 | 1351 |
<I/σ(I)> | 18.3 | |
Completeness [%] | 98.5 | |
Redundancy | 6.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 3350, KCl |