8JY9
Crystal Structure of Intracellular B30.2 Domain of VpBTN3 in Complex with HMBPP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | LIQUID ANODE |
Source details | BRUKER METALJET |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-02-28 |
Detector | Bruker PHOTON III |
Wavelength(s) | 1.34138 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.928, 67.462, 134.597 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.390 - 1.830 |
R-factor | 0.1901 |
Rwork | 0.188 |
R-free | 0.24180 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5zxk |
RMSD bond length | 0.009 |
RMSD bond angle | 1.554 |
Data reduction software | SAINT |
Data scaling software | SAINT |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.390 | 1.860 |
High resolution limit [Å] | 1.830 | 1.830 |
Rmerge | 0.123 | 0.481 |
Number of reflections | 36047 | 1632 |
<I/σ(I)> | 13.45 | |
Completeness [%] | 99.6 | |
Redundancy | 10.07 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1 M Bis Tris pH 5.5, 2.0 M ammonium sulfate |