8J48

Crystal structure of OY phytoplasma SAP05 in complex with AtGATA18

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	80
Detector technology	PIXEL
Collection date	2022-11-27
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	1.2828
Spacegroup name	P 1 21 1
Unit cell lengths	35.835, 73.397, 58.671
Unit cell angles	90.00, 107.22, 90.00

Refinement procedure

Resolution	36.700 - 1.940
Rwork	0.202
R-free	0.23650
Structure solution method	SAD
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHENIX
Refinement software	PHENIX ((1.17.1_3660: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	36.700	2.010
High resolution limit [Å]	1.940	1.940
Rmerge	0.133	1.006
Number of reflections	20865	1747
<I/σ(I)>	10.79	1.65
Completeness [%]	97.2
Redundancy	6.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.2 M Lithium acetate dihydrate, 20% (wt/vol) polyethylene glycol 3,350