8IXT
Rat Transcobalamin in Complex with Glutathionylcobalamin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B1 |
Synchrotron site | SPring-8 |
Beamline | BL26B1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-10-13 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 51.100, 55.060, 143.670 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.450 - 1.200 |
R-factor | 0.1609 |
Rwork | 0.161 |
R-free | 0.17050 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.991 |
Data reduction software | XDS (JAN 10 2022) |
Data scaling software | XSCALE (JAN 10 2022) |
Phasing software | HKL2Map (0.4.e-beta) |
Refinement software | PHENIX (1.20-4459) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 37.500 | 43.700 | 1.230 |
High resolution limit [Å] | 1.200 | 5.370 | 1.200 |
Rmerge | 0.090 | 0.042 | 1.770 |
Rmeas | 0.092 | 0.043 | 1.798 |
Number of reflections | 127252 | 1604 | 9213 |
<I/σ(I)> | 22.44 | 84.5 | 2.25 |
Completeness [%] | 99.9 | ||
Redundancy | 43.7 | ||
CC(1/2) | 1.000 | 1.000 | 0.785 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 20 % PEG 3000 0.1M Sodium citrate pH 5.5 |