8IS7
CrtMLIKE with two FsPP molecules.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-04-15 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9794 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 50.338, 64.469, 171.061 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.230 - 1.600 |
R-factor | 0.1772 |
Rwork | 0.176 |
R-free | 0.20560 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.035 |
Data scaling software | HKL-3000 |
Refinement software | PHENIX ((1.18.2_3874: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.069 | 0.303 |
Number of reflections | 36445 | 1773 |
<I/σ(I)> | 30.75 | |
Completeness [%] | 94.1 | |
Redundancy | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M Tris, 30% PEG 4000, 0.2M MgCl2, pH 8.5 |