8IR0
AfFer mutant-P156F
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-01-02 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 116.513, 116.513, 206.664 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.650 - 2.890 |
R-factor | 0.1902 |
Rwork | 0.185 |
R-free | 0.23430 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.120 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX (1.18.2_3874) |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.650 | 2.950 |
High resolution limit [Å] | 2.890 | 2.900 |
Rmerge | 0.519 | |
Number of reflections | 16300 | 16300 |
<I/σ(I)> | 2 | |
Completeness [%] | 99.7 | |
Redundancy | 12.7 | |
CC(1/2) | 0.972 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100 mM MES, 20%(v/v) 1,4-butanediol, 200 mM Lithium sulfate, pH 6.0 |