8IQY
Asterias forbesii ferritin mutant-P156H
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-01-02 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | I 4 2 2 |
Unit cell lengths | 116.934, 116.934, 206.539 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.560 - 2.100 |
R-factor | 0.1654 |
Rwork | 0.165 |
R-free | 0.18290 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.788 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX (1.18.2_3874) |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.560 | 2.140 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 42226 | 42226 |
<I/σ(I)> | 2.7 | |
Completeness [%] | 99.7 | |
Redundancy | 13 | |
CC(1/2) | 0.943 | 0.938 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100 mM imidazole, 15%(v/v) reagent alcohol, 200 mM magnesium chloride |