8HCS
zebrafish IRF-11 DBD
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 298.15 |
Detector technology | CCD |
Collection date | 2020-10-26 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9791 |
Spacegroup name | P 43 3 2 |
Unit cell lengths | 101.324, 101.324, 101.324 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.570 - 2.750 |
R-factor | 0.237 |
Rwork | 0.233 |
R-free | 0.27410 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2irf |
RMSD bond length | 0.009 |
RMSD bond angle | 1.225 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX (1.19.2_4158) |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.570 | 2.650 |
High resolution limit [Å] | 2.550 | 2.550 |
Number of reflections | 8495 | 303 |
<I/σ(I)> | 36.4 | |
Completeness [%] | 90.2 | |
Redundancy | 2 | |
CC(1/2) | 1.000 | 0.747 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289.15 | 1.26 M sodium phosphate monobasic, 0.14 M potassium phosphate dibasic, pH 5.6 |